The OPARA service was recently upgraded to a new technical platform. You are visiting the outdated OPARA website. Please use https://opara.zih.tu-dresden.de/ for new data submissions. Previously stored data will be migrated in near future and then the old version of OPARA will finally be shut down. Existing DOIs for data publications remain valid.
X-ray tomography scan of partially dewatered filter cake
Subtitle: fully saturated and dewatered filter cake
Metadata
| Additional title | Subtitle: fully saturated and dewatered filter cake | |
| Alternative existing references for this dataset | CF_035_055200_023 filtration | |
| Alternative existing references for this dataset | CF_035_055200_023 irreducible saturation | |
| Other contributing persons, institutions or organisations | Peuker, Urs Alexander - Technical University Bergakademie Freiberg - Institute of Mechanical Process Engineering and Mineral Processing - Supervisor | |
| Other contributing persons, institutions or organisations | Leißner, Thomas - Technical University Bergakademie Freiberg - Institute of Mechanical Process Engineering and Mineral Processing - Supervisor | |
| Other contributing persons, institutions or organisations | German Research Foundation - Sponsor | |
| Other contributing persons, institutions or organisations | Esser, Simon - Technical University Bergakademie Freiberg - Institute of Mechanical Process Engineering and Mineral Processing - Researcher | |
| Person(s) who is (are) responsible for the content of the research data | Löwer, Erik - Technical University Bergakademie Freiberg - Institute of Mechanical Process Engineering and Mineral Processing (ORCID: 0000-0002-6956-8054) | |
| Description of further data processing | automatic centre shift, beam hardening correction (factor 0.05), gauss smoothing filter (kernel 0.7) | |
| Type of data acquisition | Experiment: in-situ filtration and dewatering (downscaled pressure nutsch 5 mm diameter) according VDI 2762-2 and VDI 2762-3 | |
| Used research instruments or devices | X-ray microscope (ZEISS Xradia Versa 510) | |
| Research objects | Substance: glycerol (manufacturer: Carl Roth, > 99,8 %, 24 m.-%) | |
| Research objects | Substance: potassium iodide (manufacturer: Carl Roth, > 99 %, 25 mmol/l) | |
| Research objects | Substance: gamma-Al2O3 (manufacturer: Almatis, solid powder, 55...200 µm) | |
| Abstract | X-ray tomography image of a partially dewatered filter cake. The initial slurry contains Al2O3 particles suspended in a potassium iodide-glycerol solution. These were separated by cake-forming filtration followed by dewatering. All filtration and dewatering experiments took place in an in situ apparatus within the Zeiss Xradia 510 X-ray microscope. The filter cake is dewatered until the minimum degree of saturation is reached within the pore space. A scan is taken at the equilibrium state before and after dewatering. | |
| Applied methods and techniques | VDI 2762-1, VDI 2762-2 and VDI 2762-3 | |
| Additional descriptive information to understand the data | see note parameter.png in each measurement file for further measurement and reconstruction parameters | |
| Series information | fully saturated ('filtration') and dewatered state ('irreducible saturation') | |
| Table of contents | CF_035_055200_023 (in-situ filtration and dewatering, fully saturated and dewatered state, total filter cake) | |
| Additional keywords | cake filtration, cake dewatering, X-ray tomography, in-situ, VDI 2762, capillary pressure curve, modelling | |
| Language | eng | |
| Year or period of data production | 2019 | |
| Publication year | 2021 | |
| Publisher | Technical University Bergakademie Freiberg - Institute of Mechanical Process Engineering and Mineral Processing | |
| References on related materials | IsSourceOf: 10.1016/j.seppur.2020.117854 (DOI) | |
| Content of the research data | Dataset: X-ray tomography scans of partially dewatered filter cake (.tiff stacks) | |
| Holder of usage rights | Technical University Bergakademie Freiberg - Institute of Mechanical Process Engineering and Mineral Processing | |
| Usage rights of the data | CC-BY-4.0 | |
| Software | Resource Production: Xradia XMReconstructor 11.1 | |
| Additional precise description of discipline | mechanical process engineering - solid-liquid separation - cake filtration and dewatering | |
| Discipline(s) | Engineering | de |
| Title of the dataset | X-ray tomography scan of partially dewatered filter cake |
Files in this item
This item appears in the following Collection(s)
-
Publication D: Network model of porous media – Review of old ideas with new methods [1]
The paper takes up the old ideas of describing porous media with several tube and network models. The wellknown models received from literature gave a good concept of dewatering equilibria resulting in capillary pressure curves and pore size distributions (PoSD). However, numerical methods and measurement techniques were not sophisticated allowing to evaluate the models appropriately. In this work, a numerical method based on statistics is introduced to validate the network model of FATT from 1956: The porous filter cake structure is implemented as a matrix, which elements represent the pore size correlating with the capillary entrance pressure for each pore. The input for the calculations can be any mathematical approximation of a PoSD, which can be derived from capillary pressure tests or micro computer tomography (μCT) analysis of the filter cake. A procedure based on the concept of FATT is presented to generate dewatering equilibria for different applied pressures. Therefore, the elements of the matrix are checked to be ‘dewatered’ regarding to their size, position, the applied pressure level and the progress of dewatering. The network model known from literature is improved by implementing additional conditions for the description of physical phenomena, such as the formation of residual bridge liquid or hydrodynamic isolated areas. X-ray microscopy, mercury intrusion tests and laboratory desaturation experiments by using semipermeable membranes for capillary pressure tests are used to validate the pore size distribution. The different results are integrated into the matrix model as starting parameters. For the laboratory experiments, the PoSD is calculated from the measured capillary pressure curve, using the distributed tube model and the YOUNG-LAPLACE-equation on an equal basis to the established mercury intrusion analysis. However, with the tomography measurements, it is possible to determine PoSD using different defined geometry elements fitting inside the pore space. The force balance is evaluated at the pore entrance by using the wetting line of the pore throat. The direct measurement of the void geometry allows the calculation of the pressure distribution without the LAPLACIAN assumptions. In this way, the difference between experimental, measured and modelled PoSDs is emphasised to validate the old (and improved) ideas of network models describing porous media