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X-ray tomography scan of partially dewatered filter cake
Subtitle: fully saturated and dewatered filter cake
Metadaten
| Ergänzende Titel | Subtitle: fully saturated and dewatered filter cake | |
| Alternative existierende Referenzen für den Datensatz | CF_035_055200_023 filtration | |
| Alternative existierende Referenzen für den Datensatz | CF_035_055200_023 irreducible saturation | |
| Weitere mitwirkende Personen, Institutionen oder Unternehmen | Peuker, Urs Alexander - Technical University Bergakademie Freiberg - Institute of Mechanical Process Engineering and Mineral Processing - Supervisor | |
| Weitere mitwirkende Personen, Institutionen oder Unternehmen | Leißner, Thomas - Technical University Bergakademie Freiberg - Institute of Mechanical Process Engineering and Mineral Processing - Supervisor | |
| Weitere mitwirkende Personen, Institutionen oder Unternehmen | German Research Foundation - Sponsor | |
| Weitere mitwirkende Personen, Institutionen oder Unternehmen | Esser, Simon - Technical University Bergakademie Freiberg - Institute of Mechanical Process Engineering and Mineral Processing - Researcher | |
| Für den Inhalt der Forschungsdaten verantwortliche Person(en) | Löwer, Erik - Technical University Bergakademie Freiberg - Institute of Mechanical Process Engineering and Mineral Processing (ORCID: 0000-0002-6956-8054) | |
| Beschreibung der weiteren Datenverarbeitung | automatic centre shift, beam hardening correction (factor 0.05), gauss smoothing filter (kernel 0.7) | |
| Art der Erhebung der Daten | Experiment: in-situ filtration and dewatering (downscaled pressure nutsch 5 mm diameter) according VDI 2762-2 and VDI 2762-3 | |
| Verwendete Forschungsinstrumente | X-ray microscope (ZEISS Xradia Versa 510) | |
| Zugrundeliegende Forschungsobjekte | Substance: glycerol (manufacturer: Carl Roth, > 99,8 %, 24 m.-%) | |
| Zugrundeliegende Forschungsobjekte | Substance: potassium iodide (manufacturer: Carl Roth, > 99 %, 25 mmol/l) | |
| Zugrundeliegende Forschungsobjekte | Substance: gamma-Al2O3 (manufacturer: Almatis, solid powder, 55...200 µm) | |
| Kurzbeschreibung | X-ray tomography image of a partially dewatered filter cake. The initial slurry contains Al2O3 particles suspended in a potassium iodide-glycerol solution. These were separated by cake-forming filtration followed by dewatering. All filtration and dewatering experiments took place in an in situ apparatus within the Zeiss Xradia 510 X-ray microscope. The filter cake is dewatered until the minimum degree of saturation is reached within the pore space. A scan is taken at the equilibrium state before and after dewatering. | |
| Angewendete Methoden oder Verfahren | VDI 2762-1, VDI 2762-2 and VDI 2762-3 | |
| Weitere erklärende Angaben zu den Daten | see note parameter.png in each measurement file for further measurement and reconstruction parameters | |
| Informationen zur Serie | fully saturated ('filtration') and dewatered state ('irreducible saturation') | |
| Inhaltsverzeichnis | CF_035_055200_023 (in-situ filtration and dewatering, fully saturated and dewatered state, total filter cake) | |
| Weitere Schlagwörter | cake filtration, cake dewatering, X-ray tomography, in-situ, VDI 2762, capillary pressure curve, modelling | |
| Sprache | eng | |
| Entstehungsjahr oder Entstehungszeitraum | 2019 | |
| Veröffentlichungsjahr | 2021 | |
| Herausgeber | Technical University Bergakademie Freiberg - Institute of Mechanical Process Engineering and Mineral Processing | |
| Referenzen auf ergänzende Materialien | IsSourceOf: 10.1016/j.seppur.2020.117854 (DOI) | |
| Inhalt der Forschungsdaten | Dataset: X-ray tomography scans of partially dewatered filter cake (.tiff stacks) | |
| Inhaber der Nutzungsrechte | Technical University Bergakademie Freiberg - Institute of Mechanical Process Engineering and Mineral Processing | |
| Nutzungsrechte des Datensatzes | CC-BY-4.0 | |
| Eingesetzte Software | Resource Production: Xradia XMReconstructor 11.1 | |
| Nähere Beschreibung der/s Fachgebiete/s | mechanical process engineering - solid-liquid separation - cake filtration and dewatering | |
| Angabe der Fachgebiete | Engineering | de |
| Titel des Datensatzes | X-ray tomography scan of partially dewatered filter cake |
Dateien zu dieser Ressource
Die Datenpakete erscheinen in:
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Publication D: Network model of porous media – Review of old ideas with new methods [1]
The paper takes up the old ideas of describing porous media with several tube and network models. The wellknown models received from literature gave a good concept of dewatering equilibria resulting in capillary pressure curves and pore size distributions (PoSD). However, numerical methods and measurement techniques were not sophisticated allowing to evaluate the models appropriately. In this work, a numerical method based on statistics is introduced to validate the network model of FATT from 1956: The porous filter cake structure is implemented as a matrix, which elements represent the pore size correlating with the capillary entrance pressure for each pore. The input for the calculations can be any mathematical approximation of a PoSD, which can be derived from capillary pressure tests or micro computer tomography (μCT) analysis of the filter cake. A procedure based on the concept of FATT is presented to generate dewatering equilibria for different applied pressures. Therefore, the elements of the matrix are checked to be ‘dewatered’ regarding to their size, position, the applied pressure level and the progress of dewatering. The network model known from literature is improved by implementing additional conditions for the description of physical phenomena, such as the formation of residual bridge liquid or hydrodynamic isolated areas. X-ray microscopy, mercury intrusion tests and laboratory desaturation experiments by using semipermeable membranes for capillary pressure tests are used to validate the pore size distribution. The different results are integrated into the matrix model as starting parameters. For the laboratory experiments, the PoSD is calculated from the measured capillary pressure curve, using the distributed tube model and the YOUNG-LAPLACE-equation on an equal basis to the established mercury intrusion analysis. However, with the tomography measurements, it is possible to determine PoSD using different defined geometry elements fitting inside the pore space. The force balance is evaluated at the pore entrance by using the wetting line of the pore throat. The direct measurement of the void geometry allows the calculation of the pressure distribution without the LAPLACIAN assumptions. In this way, the difference between experimental, measured and modelled PoSDs is emphasised to validate the old (and improved) ideas of network models describing porous media