Technische Universität Bergakademie Freiberg
Permanent URI for this communityhttp://opara.zih.tu-dresden.de/handle/123456789/16
Research data repository of Freiberg University of Mining and Technology.
Browse
Browsing Technische Universität Bergakademie Freiberg by Title
Now showing 1 - 20 of 95
- Results Per Page
- Sort Options
Item Open Access 2D Imaging Simulation from 3D Particle Data: Extended Python Notebooks, Simulation Results(Technische Universität Bergakademie Freiberg, 2024-07-30) Buchwald, Thomas2D projection imaging techniques are simulated with 3D particle data from tomography measurements. This submission contains two distinct parts: Python notebooks to simulate 2D imaging of the particles, and the resulting simulation dataset. This dataset extends a previous one (https://doi.org/10.25532/OPARA-479) by an additional method of particle surface area determination and a larger dataset of randomly oriented projections – ten instead of the previous three. The Python notebooks were created with Jupyter Lab and Anaconda. A environment.yml file is provided that recreates the Anaconda environment. The simulation dataset that results from the provided Python notebooks is made available as CSV files or as pickled Python (pandas) DataFrames. Please refer to the included Readme for a detailed description of the files contained in the archive.Item Open Access 2D Imaging Simulation from 3D Particle Data: Python Notebooks, Particle Datasets, and Simulation Results(Technische Universität Bergakademie Freiberg, 2024-05-14) Buchwald, Thomas; Ditscherlein, Ralf2D projection imaging techniques are simulated with 3D particle data from tomography measurements. This submission contains three distinct parts: original particle data, Python notebooks to simulate 2D imaging of the particles, and the resulting simulation dataset. The particle data comes as STLs that have been converted from VTK particle data as provided by the PARROT database (https://parrot.tu-freiberg.de/). The STL files are *not* identical with the STLs provided by PARROT as of May 2024! The particle data folder is provided as separate archive because of its large size. The Python notebooks were created with Jupyter Lab and Anaconda. A environment.yml file is provided that recreates the Anaconda environment. The simulation dataset that results from the provided Python notebooks is made available as CSV files or as pickled Python (pandas) DataFrames. Please refer to the included Readme for a detailed description of the files contained in the archive.Item Open Access 3 tomographic data sets of nano-CT measurements of a 30:70 vol-% mixture of talcum and saxolite(Technische Universität Bergakademie Freiberg, 2022-09-02) Ditscherlein, RalfAll 3 data sets are sub-volumes (Field of View approx. 65 µm) of a total sample of a particle mixture of talc and saxolite fixed in a matrix by means of epoxy resin and spacer particles (nanometre-sized carbon black particles, 150 nm equivalent spherical diameter). The primary analysis was carried out using nano-CT. The reconstructed result data are stored in the form of TIF files as sectional images (folder "rotated"). In addition, a correlation was carried out by means of EDXS analytics, the chemical information of which was used to train a segmentation algorithm. Since EDXS analysis requires a planar surface, the sample was further processed using FIB. The divergence of the ion beam produces a slight angular deviation from the perpendicular of the nano-CT volume, which necessitated a rotation of the initial volume data (--> "rotated"). The correlated result data of the particle-discrete phase information are also stored ("rotated segmented").Item Open Access Additional data: Impact of Chitosan's Degree of Deacetylation, Molecular Weight, and Crystallinity on the Photoresponsive Properties of Azobenzene-modified Films and Membranes.(Technische Universität Bergakademie Freiberg, 2024-11-15) von Seggern, Nils; M. Thiebes, Yannick; Niewa, Rainer; Cord-Landwehr, Stefan; Moerschbacher, Bruno; Tovar, Günter E.M.; Stegbauer, LinusA profound understanding of how the degree of deacetylation (DDA), polymerization degree (DP) and photoswitch concentration impact the photomodulation of properties of chitosan(CS)-based responsive materials can serve as a framework for future applications. Herein, we report responsive thin-films manufactured from chitosans with DDA ranging from 70-94% and DP between 170-3380, incorporating 10 30mol% of the light-responsive azobenzene derivative Sodium-4-[(4-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)phenyl)diazenyl]-benzenesulfonate (TEGABS). During UV-irradiation of the 10 30% TEGABS|CS thin-films, e.g. a significant increase of the indentation modulus by 10 ± 5% is observed. UV illumination leads to a decrease of the water vapor permeability (WVP), reducing it by up to 81 ± 17% compared to native state. We demonstrate that TEGABS up to 10% remains as a solid-solution in CS films with differing amount of H-aggregates depending on the DDA and DP. TEGABS in concentrations >10% in CS leads to phase separation of TEGABS crystallites with a diameter of 21 ± 8 nm. To conclude the photothermal heating by UV irradiation and the resulting water evaporation are identified as the primary driving force for the variation in mechanical properties and WVP, with photoisomerization playing a subordinate factor. These findings provide a new pathway for the design of polysaccharide-based water vapor permeable photoresponsive membranes.Item Open Access Colloidal probe atomic force microscopy measurements on pristine gas bubbles, agglomerates and particle-laden gas bubbles(Technische Universität Bergakademie Freiberg, 2024-07-08) Nicklas, JanThis dataset contains experimental Atomic Force Microscopy (AFM) force-displacement measurements of poorly wetted alumina particles (colloidal probes) < 15 µm interacting with pristine gas bubbles, agglomerates and particle-laden gas bubbles (hetero-coagulates) in an aqueous environment. The data was generated in the context of the Collaborative Research Center CRC 920 (Project ID 169148856 – subproject B04) that is funded by the German Research Foundation (DFG). The data set is of interest for researches that study the agglomeration or hetero-coagulation in liquid environment, and it is expected to be of particular interest to those that are concerned with the simulation and modeling of these processes (for example by Discrete Element Method). The AFM raw data was baseline corrected to increase the accessibility of the data sets to those less familiar with the AFM. A detailed interpretation of the AFM data in this repository is found in https://doi.org/10.1021/acs.langmuir.3c01781 and https://doi.org/10.1016/j.colsurfa.2024.134660.Item Open Access Controlling structural instability in the Cu$_{12-x}$Ni$_x$Sb$_4$S$_{13}$ ($x$\,=\,0, 0.05, 0.2, 0.5) tetrahedrites(Technische Universität Bergakademie Freiberg, 2026-01-08) Bolielyi, Oleksandr; Dobrozhan, Oleksandr; Levytskyi, Volodymyr; Tsirlin, Alexander A.; Pshenychnyi, Roman; Leithe-Jasper, Andreas; Gumeniuk, RomanCu$_{12-x}$Ni$_x$Sb$_4$S$_{13}$ ($x\,=\,0, 0.05, 0.2, 0.5$) tetrahedrites were synthesized by the polyol method. Measurements of magnetic susceptibility, specific heat capacity as well as electrical and thermal transport properties indicated a structural phase transition (SPT) of 1$^{\mathrm{st}}$ order at $T_k\,=\,75-85$\,K, which is accompanied by strong changes in electronic density of states (EDOS) and entropy for $x\,=\,0, 0.05, 0.2$ whereas only weak changes were observed at $x\,=\,0.5$. However, further temperature dependent synchrotron high-resolution powder X-ray diffraction (HR PXRD) studies indicated compounds with Ni-content $x\,=\,0$ and 0.5 to remain body-centered cubic [space group (SG) $I\bar{4}3m$, $a\,\approx\,10.4(1)$\,\AA] down to 10\,K, whereas crystal structures of $x\,=\,0, 0.05$ and 0.2 became tetragonal, (SG $P\bar{4}c2$, $a_\mathrm{tetr}\,\approx\,a_\mathrm{cub}\sqrt{2}$, $c_\mathrm{tetr}\,\approx\,a_\mathrm{cub}$) below $T_k$. Comparing changes of EDOS at the Fermi level [$\Delta N^{(E_\mathrm{F})}$] deduced from magnetic and thermodynamic data with those calculated from density functional theory (DFT) assuming the validity of the rigid-band approximation, we found $\Delta N^{(E_\mathrm{F})}_\mathrm{theor}\,\approx\,0$ when compared with cubic and tetragonal arragements for Cu$_{11.5x}$Ni$_{0.5}$Sb$_4$S$_{13}$, which indicate the latter to be unstable. This study shows that SPT in tetrahedites is facilitated by the presence of minor amount of a dopant.Item Open Access Correlation Velocimetry inside a model of the human airways(Technische Universität Bergakademie Freiberg, 2025-02-07) Bauer, Katrin; Kluwe, Moritz NiklasThe dataset corresponds to the publication "Deterministic periodic structures in a model of the human airways" by Kluwe et al. 2025. It contains raw data obtained from an optical setup used for point-wise velocity measurements using Correlation Velocimetry in a model of human airways. The recorded data consists of stereo audio files sampling the photo-electric response of two photodiodes to the passage of tracer particles. The time lag between both signals corresponds to the mean time of flight of ensembles of particles between both detectors. Using the known distance between the detectors (272 micrometers), the mean velocity of the tracer particles can be calculated. This dataset includes the raw data evaluated and discussed in the publication.Item Open Access Correlative X-ray micro-Computed Tomography (X-µCT) scans of Engineered Artificial Minerals (EnAM)(Technische Universität Bergakademie Freiberg, 2024-11-07) Siddique, Asim; Schröer, LaurenzCharacterizing complex particulate materials like slag using X-ray microcomputed tomography (μCT) is challenging due to minimal grey-scale contrast from similar attenuation properties among phases and intricate microstructures. To address this problem, we developed a standardized multi-scale correlative methodology that combines μCT at different resolutions with scanning electron microscopy and energy-dispersive X-ray spectroscopy (SEM-EDS) and X-ray fluorescence (XRF). By scanning large samples for statistical significance and sub-samples at higher resolutions, we capture detailed microstructures. Aligning SEM-EDS data with μCT scans using inherent markers enables accurate phase segmentation. Mineral mapping from SEM-EDS can help to train segmentation models for μCT data, overcoming μCT limitations and allowing precise 3D mineralogical characterization. This approach provides a robust framework for analyzing complex slag particles. This project has received funding from the European Union's Horizon 2020 research and innovation programme under grant agreement No 101005611 https://excite-network.eu.Item Open Access Data Archive DFDP Seismic extended 3D surface and VSP survey (Alpine Fault 3D-VSP)(Technische Universität Bergakademie Freiberg, 2021-03-29) Buske, Stefan; Benson, Adrian; Lindsay, Danielle; Lawton, Don; Gulley, Anton; Lepine, Patrick; Constantinou, Alexis; Savage, Martha; Bowman, Hamish; Kofman, Randolf; Kellett, Richard; Mann, Christin; Lay, Vera; Schmitt, Douglas; Hopp, Chet; Townend, John; Kleine, Franz; Bertram, Malcolm; Eccles, Jennifer; Gorman, Andrew; McNab, Andrew; Hall, Kevin; Bodenburg, Sascha BarbaraThis seismic data set was acquired in 2016 by a joint effort of several partners. Within this archive, we provide the coordinate lists and correlated data with local coordinates. A detailed field report by Townend et al. (2016) describes the field procedures and available data. Please see the included pdf-file for more details.Item Open Access Dataset for "CFD Analysis of Mucus Bridge Instability and Breakup in the Vocal Folds"(Technische Universität Bergakademie Freiberg, 2025-08-22) Heinrich, MartinThis dataset accompanies the research paper: Heinrich, M., Döllinger, M., and Schwarze, R. (2026). CFD Analysis of Mucus Bridge Instability and Breakup in the Vocal Folds. Physical Review Fluids, 11. https://doi.org/10.1103/qq23-l918. The archive contains OpenFOAM case setups, simulation scripts, and extracted visualization data for the multiphase Volume-of-Fluid CFD simulation of mucus bridge breakup during vocal fold phonation.Item Open Access Dataset Supporting the Characterization of Slag from SOEL Interconnect Remelting(Technische Universität Bergakademie Freiberg, 2025-08-13) Mongoljiibuu, Shine-OdThis dataset supports the manuscript titled “Chromium in Slag from SOEL Interconnects Remelting: Characterization and Recycling Potential”. The study focuses on characterizing the bulk composition, mineralogy, its distribution, and elemental distributions in slag generated during the remelting of Solid Oxide Electrolyzer (SOEL) interconnects. The data include X-ray Fluoroscence (XRF) data, X-ray Diffraction (XRD) pattern data, X-ray Computed Tomography (XCT) dataset, and Scanning Electron Microscopy (SEM)-based Mineral Liberation Analysis dataset.Item Public Metadata DFG 465144480: Boron-free self-glazing Al₂O₃-C refractories(Technische Universität Bergakademie Freiberg, 2026-04-01) Roungos, Vasileios; Gehre, Patrick; Salpagarov, Eldar; Aneziris, Christos G.Al₂O₃-C refractories are extensively used as functional components in the continuous casting of steel. These high-duty products such as submerged entry nozzles, ladle shrouds, and monoblock stoppers contain up to 30 wt.-% carbon and present excellent mechanical, thermal and chemical properties, enabling the cost- and quality-effective implementation of the continuous casting process. Ceramic glazes are externally applied on Al₂O₃-C flow control refractory products to protect carbon from oxidation. These glazes typically contain boron. However, the increasing requirements for clean steel technology along with environmental- and health issues associated with boron compounds will make the utilization of boron-free glazes a necessity in the upcoming years. New boron-free self-glazing Al₂O₃-C formulations with sodium carbonate, wollastonite and magnesia additives were developed with the assistance of the FactSage software tool. These compositions presented a softening point in the range of 1000-1100 °C for self-glaze formation, which is the typical preheating temperature range for Al₂O₃-C functional refractory products. In addition, the influence of particle packing on their oxidation resistance was investigated, based on established particle size distribution models.Item Public Metadata DFG 465144480: Impact of cyclic CIP on the oxidation resistance and physical properties of a newly developed boron-free self-glazing Al2O3-C refractory(Technische Universität Bergakademie Freiberg, 2026-03-31) Roungos, Vasileios; Gehre, Patrick; Brachhold, Nora; Fischer, Undine; Aneziris, Christos G.The impact of cyclic cold isostatic pressing (C-CIP) on the oxidation resistance and physical properties of a boron-free self-glazing Al2O3-C refractory for steel casting applications was investigated. Pulsations with amplitudes of 20, 40 and 65 MPa were thereby applied either at maximum isostatic pressure or at increasing pressure. The maximum isostatic pressures applied were 80, 100 and 150 MPa, respectively. Both cycling pressurizations improved the oxidation resistance and physical properties. Higher densities were obtained at higher cycling amplitudes, in particular when the pulsations were applied at maximum isostatic pressure. In addition, the evolution of a broader pore size distribution with peaks at pores larger than 4 μm was found. The pore size distributions of the samples pressed by C-CIP at increasing pressure were narrower, with higher peaks at smaller pore sizes in the area of 2.5 μm. It was shown that utilizing cycling pressurization enables tailoring of pore sizes in carbon-bonded refractories as well, providing a powerful tool for the material design of refractories.Item Open Access Digital Supplement Michael Hohf, Dissertation (Tourmaline chemistry & Geochronology Río Blanco-Los Bronces, Chile)(Technische Universität Bergakademie Freiberg, 2021-05-29) Ratschbacher, Lothar13 datafiles, Supplement zur Dissertation Michael Hohf (Rohdaten der U-Pb und Ar/Ar Geochronologie; Mineralchemie der Tourmalinanalysen, Bor- und Schwefel-Isotopen-Daten; Karten)Item Open Access Dynamic Image Analysis: Python Notebooks, Particle Datasets, and Simulation Results(Technische Universität Bergakademie Freiberg, 2024-08-20) Buchwald, ThomasThis submission serves as a validation dataset for the simulation results of 2D imaging methods from 3D particle meshes. The submission contains dynamic image analysis data that can be used for validation of simulation results, Python notebooks for extraction of particles and calculation of particle characteristics, and the final results in as pickled Pandas DataFrames and CSV files. This dataset extends to previous submission: https://doi.org/10.25532/OPARA-479 and https://doi.org/10.25532/OPARA-587, which contain the 3D particle dataset and the simulation algorithm notebooks.Item Open Access Epoxy-Based Particle Sample Preparation with Nano-Graphite as Spacer - RAW Data (Particle Sample Preparation) - Different mixtures (by volume) of graphite-nanoparticles and analysis particles(Technische Universität Bergakademie Freiberg, 2020-05-08) Ditscherlein, RalfTo get good image segmentation results in tomographic analysis methods, particles has to be seperated from each other while embedding them into a matrix. Low X-ray absorbing nano-graphite below the voxel resolution of the system is mixed with the analysis particles to form a shell to avoid direct particle-particle contact. After mixing it with epoxy resin, the paste is sucked into a polymeric tube of 2 mm inner diameter. After hardening, the formed cylinder was scanned with an X-ray microscope (ZEISS Xradia Versa 510) with the following parameters: 80 keV, 7 W, 360°, 2001 projections, 1 s exposure time, 2 µm voxel size, binning 2. After scannning, the following filters were applied while reconstruction with ZEISS reconstructor: Beam Hardening Correction 0.05, Smoothing 0,7. Detailed overview of the parameters is summarized as screenshots within the repository. To determine an optimal mixture of the two components, the following volume-fractions were analysed: Nanoparticle:Particle 20vol-%:80vol-% 40vol-%:60vol-% 60vol-%:40vol-%Item Open Access Experimental Cake Filtration Data and Code for Analysis, Graph Generation(Technische Universität Bergakademie Freiberg, 2021-12-08) Buchwald, ThomasThis collection belongs to the doctoral thesis "Nonlinear Parameter Estimation of Experimental Cake Filtration Data". Most of the content are Jupyter notebooks which contain the Python code which reproduces graphs found in the thesis from the original experimental data. The lab practice dataset that contains 500 filtration experiments is contained in the folder for section 3.5. The notebooks are not strictly sorted by section. At any rate, the Readme will guide you to the notebook which produces a certain graph, if it is not part of the main notebook of that specific section. The original Python environment was set up with Anaconda. Please use the provided .yml file to create a Python environment which contains all the necessary packages. Some notebooks may not work with the most current versions of the packages, so updating is not necessarily a good idea.Item Open Access Filtration and Particle Discrete Data (glass beads < 160 µm) for 'Project Development of multivariant structure and process models for filter cakes, combining experimental methods of process engineering with digital computer based methods'(Technische Universität Bergakademie Freiberg, 2026-04-29) Löwer, ErikThis dataset contains primary experimental data investigating the filtration behavior and particulate properties of glass particles, spherical, < 160 µm. The data was generated through separation tests conducted in accordance with the VDI 2762 guideline (cake-forming filtration). The study aims to correlate particle morphology with specific filter cake resistance within a viscous medium. Soda-lime glass (SiO2, 2.55 g/cm³) from Sigmund Lindner GmbH, was used as the disperse phase. To ensure a defined particle size distribution, the material was pre-classified to a target range of 70 to 160 µm using a Nisshin Turbo Classifier TC-15M fine air classifier. The continuous medium consisted of a binary water-glycerin mixture: Glycerin content: 24 mass percent (wt%) Additive: 25 mM potassium iodide (KI). Both chemicals were sourced in analytical grade from Carl Roth GmbH + Co. KG. Complementary 3D-characterization data, including CT scans (Computed Tomography) and segmented individual particle data, are archived in the "Parrot" database of the TU Bergakademie Freiberg (https://parrot.tu-freiberg.de/).Item Open Access Filtration and Particle Discrete Data (quartz < 200 µm) for 'Project Development of multivariant structure and process models for filter cakes, combining experimental methods of process engineering with digital computer based methods'(Technische Universität Bergakademie Freiberg, 2026-04-29) Löwer, ErikThis dataset contains primary experimental data investigating the filtration behavior and particulate properties of quartz particles. The data was generated through separation tests conducted in accordance with the VDI 2762 guideline (cake-forming filtration). The study aims to correlate particle morphology with specific filter cake resistance within a viscous medium. Quartz (SiO2, 2.7 g/cm³) from Strobel Quarzsand GmbH, product name BCS201, was used as the disperse phase. To ensure a defined particle size distribution, the material was pre-classified to a target range of 50 to 200 µm using a Nisshin Turbo Classifier TC-15M fine air classifier. The continuous medium consisted of a binary water-glycerin mixture: Glycerin content: 24 mass percent (wt%) Additive: 25 mM potassium iodide (KI). Both chemicals were sourced in analytical grade from Carl Roth GmbH + Co. KG. Complementary 3D-characterization data, including CT scans (Computed Tomography) and segmented individual particle data, are archived in the "Parrot" database of the TU Bergakademie Freiberg (https://parrot.tu-freiberg.de/).Item Open Access Fully saturated and dewatered filter cakes at different resolutions(2021-08-23) Löwer, ErikAppendix to Publications A to E with investigations of different particle systems (material, size and shape variation). X-ray tomography image of fully and partially dewatered filter cakes. The initial slurries contains mica, dolomite, quartz, limestone or glass particles suspended in a potassium iodide-glycerol brine. The different shaped particles were separated by cake-forming filtration followed by dewatering. All filtration and dewatering experiments took place in an in situ apparatus within the Zeiss Xradia 510 X-ray microscope. The filter cake is dewatered until the minimum degree of saturation is reached within the pore space. A scan is taken at the equilibrium state before and after dewatering. A small section in the center of the desaturated filter cakes was additionally measured at a significantly smaller field of view and higher resolution in order to be able to determine the local contact angle in addition to the saturation distribution and the size of the individual liquid bridges.